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CAS 6700-34-1 Pharmaceutical Raw Materials Dextromethorphan Hydrobromide

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CAS 6700-34-1 Pharmaceutical Raw Materials Dextromethorphan Hydrobromide

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Packaging Details : disguised package
CAS : 6700-34-1
Purity : 99%
Appearance : white powder
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CAS 6700-34-1 Pharmaceutical Raw Materials Dextromethorphan Hydrobromide


Dextromethorphan (DXM or DM) is an antitussive (cough suppressant) drug.
Dextromethorphan has also found other uses in medicine, ranging from pain relief to psychological applications. It is sold in syrup, tablet, spray, and lozenge forms. In its pure form, dextromethorphan occurs as a white powder.


Description:

Dextromethorphan Hydrobromide
Alias: Romilar
CAS No.: 125-69-9/6700-34-1
EINECS No.: 204-750-1
MF: C18H26BrNO
MW: 352.31
Purity: 98.0%
Appearance: White or kind of white crystalline powder, soluble in water.

Applications:

DXM is also used recreationally. When exceeding label-specified maximum dosages, dextromethorphan acts as a dissociative hallucinogen. Its mechanism of action is via multiple effects, including actions as a nonselective serotonin reuptake inhibitor and a sigma-1 receptor agonist. The major metabolite of DXM, dextrorphan, also acts as an NMDA receptor antagonist. In high doses this produces effects similar to, yet distinct from, the dissociative states created by other dissociative anaesthetic. As well, the metabolite 3-methoxymorphinan of dextrorphan (thus a second-level metabolite of DXM) produces local anesthetic effects in rats with potency above dextrorphan, but below that of DXM.
Product Basic Information
The primary use of dextromethorphan hydrobromide is as an antitussive, or cough suppressant. This is one of the most popular ingredients in over-the-counter cold and cough medications. This medication may be added to other preparations to help treat pain and a variety of other disturbances as well.


CERTIFICATE OF ANALYSIS
Product name
Dextromethorphan Hydrobromide
CAS No.
6700-34-1
Outer Packing
25KG /drum
Production date
2016.06.11
Shelf life
2020.06.10
Standard adopted
USP38/EP8
Items of analysis
Specification
Results
Apperance

Practically white crystal or crystalline powder
White crystalline powder
FT-IR
The sample spectrum correspond to that of the reference standard
Conforms
UV
Not more than 3.0% difference of RS(on anhydrous basis)
2.7%
Bromide Test
Yellow white precipitate forme
Conforms
Specific rotation A
1.8w/v in water:Not more than 1.0%difference of RS
0.4%
Specific rotation B
2.0%w/v in 0.1M HCL: +28℃to +30℃ at 589nm and 20℃(on anhydrous basis)
+28.4℃
Clarity of solution
5.0%w/v in alcohol:Clear and colorless
Conforms
PH
5.2-6.5(1 in 100 water solution)
5.7
Acidity or Alkalinity
Not more than 0.4ml of 0.01M HCLconsumed
0.30ml
Water(by KF Titration)
4.0%—5.5%
4.9%
impurities A,B,C,D
For each of impurities A,B,C,D not more than 0.5%
Impurities A,B,C,D; Not detected.
impurities A,B,C,D
Among impurities A,B,C,D not more than one greater than 0.25%
0
For each of unspecified impurities
not more than0.10%
﹤0.05%
Total impurities
not more than 1.0%
﹤0.05%
Residue on Ignition
Not more than 0.1%
0.08%
N,N-Dimethylaniline
Not more than 0.001%
Conforms
Phenolic compounds
No blue-green color develops
Conforms
Assay A (by HPLC)
98.0%~102.0%(on anhydrous basis)
99.9%
Assay B(by titration)
99.0%~101.0%(on anhydrous basis)
99.2%
Methanol
≤3000ppm
N.D
Toluene
≤890ppm
5.8ppm
Acetone
≤5000ppm
Conforms
Storage
Preserve in tight containers;protected from light
Conforms
Conclusion
Qualified

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